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Oligo Synthesis

Oligo Synthesis : CEPs

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2'-OMe-ibu-G-CE Phosphoramidite

2'-OMe-ibu-G-CE Phosphoramidite 5'-Dimethoxytrityl-N-isobutyryl-Guanosine,2'-O-methyl,3'-[(2-cyanoethyl)-(N,N-diisopropyl)]-phosphoramidite

Glen Research

Catalogue No.DescriptionPack SizePriceQty
10-3120-022'-OMe-ibu-G-CE Phosphoramidite0.25 g £23.00 Quantity Add to Order
10-3120-052'-OMe-ibu-G-CE Phosphoramidite0.5 g £45.00 Quantity Add to Order
10-3120-102'-OMe-ibu-G-CE Phosphoramidite1.0 g £91.00 Quantity Add to Order
10-3120-902'-OMe-ibu-G-CE Phosphoramidite100 umole £14.00 Quantity Add to Order

Description

2'-OMe-RNA Phosphoramidites

Glen Research 2'-OMe-RNA CE (β-cyanoethyl) Phosphoramidites are designed to produce synthetic oligonucleotides containing nuclease resistant 2'-O-methyl ribonucleotide linkages.  Deprotection, isolation and handling of 2'-O-methyl oligonucleotides are identical to the procedures for oligodeoxynucleotides.

 

Ultramild 2'-OMe-RNA

The use of UltraMild monomers in oligonucleotide synthesis has allowed very sensitive dyes like TAMRA, HEX and Cy5 to be used virtually routinely.  The DNA and RNA monomers are currently available and we also provide this set of 2'-OMe-RNA monomers.  In our version of this chemistry, we use as protecting groups phenoxyacetyl (Pac) for A, acetyl (Ac) for C, and isopropyl-phenoxyacetyl (iPr-Pac) for G.
It has become clear that acetic anhydride in the conventional capping mix can cause transamidation in situations where an amine protecting group is quite labile.   This leads to acetyl protection on the amino group that may be slow to be removed.  Consequently, if many dG residues are included in the oligonucleotide, we recommend the use of phenoxyacetic anhydride (Pac2O) in Cap A.  This modification removes the possibility of exchange of the iPr-Pac protecting group on the dG with acetate from the acetic anhydride capping mix.

 
Formula: C45H56N7O9P           
M.W.: 869.97 
F.W.: 359.24 

Diluent: Anhydrous Acetonitrile

Coupling: 6 minute coupling time

Deprotection: No changes needed from standard method recommended by synthesizer manufacturer.

Storage: Storage: Refrigerated storage, maximum of 2-8°C, dry

Stability in Solution: 3-5 days

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Protocols

MSDS

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References

Glen Report 19.2: New Lines Of Monomers - Ht For High Throughput And Lc For Low Cost Rn

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Applications & Benefits

DILUTION/COUPLING DATA

The table below shows pack size data and, for solutions, dilutions and approximate couplings based on normal priming procedures. Please link for more detailed usage information with the various synthesizers.

ABI 392/394
Cat.No. Pack Size Grams/ Pack 0.1M Dil. (mL) LV40 LV200 40nm 0.2µm 1µm 10µm
Approximate Number of Additions
10-3120-02 0.25grams .25grams 2.87 82.33 49.4 30.88 22.45 16.47 4.12
10-3120-05 0.5grams .5grams 5.75 178.33 107 66.88 48.64 35.67 8.92
10-3120-10 1.0gram 1grams 11.49 369.67 221.8 138.63 100.82 73.93 18.48
10-3120-90 100µmoles .087grams 1 20 12 7.5 5.45 4 1
10-3120-2HT 2grams 2grams 22.99 753 451.8 282.38 205.36 150.6 37.65
Expedite
Cat.No. Pack Size Grams/ Pack Dilution (mL) Molarity 50nm 0.2µm 1µm 15µm  
Approximate Number of Additions
10-3120-02 0.25grams .25grams 4.29 .07 79.4 49.63 36.09 4.96  
10-3120-05 0.5grams .5grams 8.58 .07 165.2 103.25 75.09 10.33  
10-3120-10 1.0gram 1grams 17.16 .07 336.8 210.5 153.09 21.05  
10-3120-90 100µmoles .087grams 1.5 .07 23.6 14.75 10.73 1.48  
10-3120-2HT 2grams 2grams 34.31 .07 679.8 424.88 309 42.49  
Mermade
Cat.No. Pack Size Grams/ Pack Dilution (mL) Molarity 30nm 200nm 1000nm    
Approximate Number of Additions
10-3120-02 0.25grams .25grams 4.29 .07 81 50.63 36.82    
10-3120-05 0.5grams .5grams 8.58 .07 166.8 104.25 75.82    
10-3120-10 1.0gram 1grams 17.16 .07 338.4 211.5 153.82    
10-3120-90 100µmoles .087grams 1.5 .07 25.2 15.75 11.45    
10-3120-2HT 2grams 2grams 34.31 .07 681.4 425.88 309.73    

 

 

 

 

 


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If you cannot find the answer to your problem then please contact us or telephone +44 (0)1954 210 200

Related products

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